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The vWF domain

Perkins &co-workers (Perkins et al. , 1994; Edwards &Perkins, 1995) used an alignment of 92 sequences together with spectroscopic data, and prediction algorithms to predict that the vWf domain would comprise a repeating arrangement of strands and helices. Edwards &Perkins combined a THREADER scan with analysis of the location of active site residues, a putative disulphide bridge, and the principles of protein 3D structure. They suggested that the vWf domain would be most likely to resemble ras p21. The subsequently determined 3D structures [Lee et al., 1995] showed this prediction of secondary structure and fold to be largely correct [Russell \& Sternberg, 1995].

Our mapping technique allows many of the features exploited by Perkins et al. to be combined in a prediction. Figure 2 shows a vWf pattern based on the prediction of Perkins &co-workers [Edwards \& Perkins, 1995][Perkins et al., 1994]. In addition to a pattern of predicted secondary structures, the pattern also contains detailed information as to the loop lengths, and details of two distance restraints: one from a pair of aspartic acids thought to be involved in a metal binding site (constrained to have their axial coordinates within 15 Å), and a putative disulphide bond (constrained to have their axial coordinates within 9.5 Å). A tolerance of Å was added to each of these restraints to allow for changes in secondary structure packing across similar protein 3D structures.

A comparison of the vWf pattern to the database of 780 domains finds Elongation factor Tu (PDB code 1ETU), Ras P21 (821P) and Che-Y (3CHY) as the three top scoring folds, with other double-wound, , Rossmann-type folds following in the top 20 scoring folds. The top 3 scoring proteins are highly similar to the recently solved structures of the vWf, with Ras P21/Elongation factor Tu being the most similar [Lee et al., 1995].



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